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Compact Split High Pressure Gas Tube Furnace (HIP)
  • Compact Split High Pressure Gas Tube Furnace (HIP)
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Compact Split High Pressure Gas Tube Furnace (HIP)

Split High Pressure Gas Tube Furnace (HIP) is a compact high pressure tube furnace featuring a Ni-based super-alloy tube vessel. This split tube furnace is a compact (hot isostatic pressure) HIP tube furnace for researching a new generation of materials at a low cost.

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  • Product Details
  • HTTF-1200-HP Split High Pressure Gas Tube Furnace (HIP) is a compact high pressure tube furnace featuring a Ni-based super-alloy tube vessel (30mm O.D x 12 mm I.D x 560 mm L). The split high pressure furnace can be used under ultra-highly oxidizing and inert gas atmosphere up to 1100°C to process special compounds. This split tube furnace is a compact (hot isostatic pressure) HIP tube furnace for researching a new generation of materials at a low cost. 

    A solenoid valve of gas tube furnace is installed on the flange allows auto-pressure relief control. Temp. Control and Pressure Real-time Monitoring software is also included. (new feature since 5/12/14, Laptop is included since 9/10/15 )

     

    Standard specification of Compact High Pressure Gas Split Tube Furnace

    Furnace Structure of vacuum gas tube   furnace

    Double-layer steel casing

    High purity fibrous alumina insulation   for Max. energy saving.

    The aluminum heat sink on processing tube   to ensure pressure flange and fitting < 60°C

    Splittable cover for changing tube at   easy

    Power

    2.5KW

    Voltage

    AC 208 - 240V Single Phase, 50/60 Hz

    Max. Temperature

    1100°C

    Heating Rate

    <= 10°C/min

    Pressure Vessel of High Pressure Tube   Furnace

    Made of Special Ni-based Superalloy: (   Waspaloy or equivalent  )

    Vessel size: 30 mm O.D x  12 mm    I.D. x 580 mm Length

    1/4NPS female fitting is installed on   both ends of flanges

    Ni-based superalloy tube vessel (30mm O.D   x 12 mm I.D x 580 mm L)

    50mm OD x 20 mm ID x  580mmL tube is available in the product   option

    Working Pressure vs temperature

    Max. 2900 PSI  (20 Mpa)        800°C

    Max. 1740 PSI  (12Mpa)         900°C

    Max. 870 PSI   (6 Mpa)     1000°C

    Max. 580 PSI   (4 Mpa)     1100°C

     

    Warning: of Compact High Pressure Gas   Tube Furnace

    Please set up a pressure alarm point in   digital pressure display before the operation

    Must install a pressure regulator on the   gas cylinder to increase pressure gradually.

    Service life depends on the maximum   operating temperature and sample used. The high-pressure vessel is a   consumable part, please order replacement once observed deformation.

    Compatible Gas and crucible Gas Tube   Furnace

    Oxygen and inert gasses such as N2, Ar   and He

    Note: Compact High Pressure split Tube   Furnace (HIP)

    Small quartz or Alumina boat should be   used to load the sample inside the vessel. Please click the link below to   order separately. Never place the sample directly onto the vessel without a   crucible. Vessel service-life could be reduced significantly if you do so.

    You may use gold or nickel foil to wrap   the crucible boat to minimize the contamination to the pressure vessel.

    Heating Zone length

    200 mm    ( single zone )

    Temperature Uniformity

    +/-1°C within 50mm and +/-2°C in 70mm

    Temperature control Split Tube Furnace

    Precision temperature controller with 30   segments programmable and PID autotune

    LED digital display with the protection   of over temperature and the thermal couple broke.

    Temperature accuracy: +/- 1°C

    K-type thermal couple built-in

    (Optional)The Eurotherm Temperature (   3000) controller is available upon request with +/- 0.1°C

    Pressure Monitoring and Relief 

    The pressure transducer is installed on   the right flange and connected to the digital pressure monitor which allows   you to set the higher pressure limit.

    One high-pressure solenoid valve is   installed on the left flange and controlled by pressure monitor.

    Max. pressure can be set on a pressure   monitor. Once Max.pressure inside vessel is reached, gas will be released   automatically. 

    Note: Max.pressure of the standard   solenoid valve is 150 bar(2165 psi/ 15MPA).    If you need pressure > 150bar at a lower temperature, the manual   valve located beneath the solenoid valve shall be shut off.

    Pressure Transducer

     

    The pressure transducer is installed on   the right flange. The pressure will be displayed in the pressure monitor on   the front panel of the furnace. Pressure measurement ranges up to 250 bars.

    The alarm system is built in the pressure   meter which allows the user to set up the high limit point of pressure. When   the measuring pressure exceeds the limit point, the alarm will be activated   and open the solenoid pressure relief valve

    Pressure Fitting Split HIP Tube Furnace

     

    Two flanges with female 1/4" NPT   fittings to connect the high-pressure tube

    One Aluminum heat radiators are installed   in front of the flange to keep flange below 100C

    One high-pressure valve is installed with   flanges

    One Pressure meter installed to one of   valve

    Two high-pressure copper gaskets are   included for immediate use.  You may   click picture below to order extra Cu gaskets

    The optional torque wrench is available   here to avoid overtightening the flange bolts

    Heating Element

    Fe-Cr-Al Alloy doped by Mo

    Application Notes   

    Hytort Application, or named   Hydroretorting of Shale Oil is a process developed by IGT to double the yield   of shale oil and hydrocarbon gasses. Please click underlined to view research   paper

    Attention: A two-stage pressure regulator   must be installed on the gas cylinder to limit the gas output pressure to the   below the safety limit. The pressure regulator is not included. Please click   here to learn how to install the gas regulator.

    Safety Notes

    Ni-based Superalloy: ( Waspaloy or   equivalent is a reliable processing tube which can be used under high temperature   and high pressure. It has excellent ductility and tensile property so only   creep deformation happens under overpressure destruction test and following   by a crack formed (usually at the hot zone at the center of the tube) to   release the pressure. Brittle fracture won’t happen in the overpressure   destruction test which means no tube explosion will happen under the   overpressure of inert gas or safe gas or under other accidents causing   overpressure of inert gas or safe gas.

    Attention: for the use of flammable,   toxic or corrosive gasses, you must contact MTI engineering group for the   consultation to know all the prerequisites and precautionary measures.

    Warning: Never put a sample inside the   tube directly without crucible or isolated foil to avoid it reacts with tube   alloy.

    Do not over-tightening the flange screws   as this may cause permanent damages to the flange or screws. Please refer to   the instructions about proper torque for installing CF flange bolts. We   recommend you use a torque wrench to tighten the screws with the flange.

    Warranty of High Pressure Furnace

    One year limited warranty (Consumable   parts such as o-rings and heating elements are not covered by the warranty,   please order the replacement at related products below.)

    Laptop, software

     


    HTTF-1200-HP Split High Pressure Gas Tube Furnace (HIP) is a compact high pressure tube furnace featuring a Ni-based super-alloy tube vessel (30mm O.D x 12 mm I.D x 560 mm L). The split high pressure furnace can be used under ultra-highly oxidizing and inert gas atmosphere up to 1100°C to process special compounds. This split tube furnace is a compact (hot isostatic pressure) HIP tube furnace for researching a new generation of materials at a low cost. 

    A solenoid valve of gas tube furnace is installed on the flange allows auto-pressure relief control. Temp. Control and Pressure Real-time Monitoring software is also included. (new feature since 5/12/14, Laptop is included since 9/10/15 )

     

    Standard specification of Compact High Pressure Gas Split Tube Furnace

    Furnace Structure of vacuum gas tube   furnace

    Double-layer steel casing

    High purity fibrous alumina insulation   for Max. energy saving.

    The aluminum heat sink on processing tube   to ensure pressure flange and fitting < 60°C

    Splittable cover for changing tube at   easy

    Power

    2.5KW

    Voltage

    AC 208 - 240V Single Phase, 50/60 Hz

    Max. Temperature

    1100°C

    Heating Rate

    <= 10°C/min

    Pressure Vessel of High Pressure Tube   Furnace

    Made of Special Ni-based Superalloy: (   Waspaloy or equivalent  )

    Vessel size: 30 mm O.D x  12 mm    I.D. x 580 mm Length

    1/4NPS female fitting is installed on   both ends of flanges

    Ni-based superalloy tube vessel (30mm O.D   x 12 mm I.D x 580 mm L)

    50mm OD x 20 mm ID x  580mmL tube is available in the product   option

    Working Pressure vs temperature

    Max. 2900 PSI  (20 Mpa)        800°C

    Max. 1740 PSI  (12Mpa)         900°C

    Max. 870 PSI   (6 Mpa)     1000°C

    Max. 580 PSI   (4 Mpa)     1100°C

     

    Warning: of Compact High Pressure Gas   Tube Furnace

    Please set up a pressure alarm point in   digital pressure display before the operation

    Must install a pressure regulator on the   gas cylinder to increase pressure gradually.

    Service life depends on the maximum   operating temperature and sample used. The high-pressure vessel is a   consumable part, please order replacement once observed deformation.

    Compatible Gas and crucible Gas Tube   Furnace

    Oxygen and inert gasses such as N2, Ar   and He

    Note: Compact High Pressure split Tube   Furnace (HIP)

    Small quartz or Alumina boat should be   used to load the sample inside the vessel. Please click the link below to   order separately. Never place the sample directly onto the vessel without a   crucible. Vessel service-life could be reduced significantly if you do so.

    You may use gold or nickel foil to wrap   the crucible boat to minimize the contamination to the pressure vessel.

    Heating Zone length

    200 mm    ( single zone )

    Temperature Uniformity

    +/-1°C within 50mm and +/-2°C in 70mm

    Temperature control Split Tube Furnace

    Precision temperature controller with 30   segments programmable and PID autotune

    LED digital display with the protection   of over temperature and the thermal couple broke.

    Temperature accuracy: +/- 1°C

    K-type thermal couple built-in

    (Optional)The Eurotherm Temperature (   3000) controller is available upon request with +/- 0.1°C

    Pressure Monitoring and Relief 

    The pressure transducer is installed on   the right flange and connected to the digital pressure monitor which allows   you to set the higher pressure limit.

    One high-pressure solenoid valve is   installed on the left flange and controlled by pressure monitor.

    Max. pressure can be set on a pressure   monitor. Once Max.pressure inside vessel is reached, gas will be released   automatically. 

    Note: Max.pressure of the standard   solenoid valve is 150 bar(2165 psi/ 15MPA).    If you need pressure > 150bar at a lower temperature, the manual   valve located beneath the solenoid valve shall be shut off.

    Pressure Transducer

     

    The pressure transducer is installed on   the right flange. The pressure will be displayed in the pressure monitor on   the front panel of the furnace. Pressure measurement ranges up to 250 bars.

    The alarm system is built in the pressure   meter which allows the user to set up the high limit point of pressure. When   the measuring pressure exceeds the limit point, the alarm will be activated   and open the solenoid pressure relief valve

    Pressure Fitting Split HIP Tube Furnace

     

    Two flanges with female 1/4" NPT   fittings to connect the high-pressure tube

    One Aluminum heat radiators are installed   in front of the flange to keep flange below 100C

    One high-pressure valve is installed with   flanges

    One Pressure meter installed to one of   valve

    Two high-pressure copper gaskets are   included for immediate use.  You may   click picture below to order extra Cu gaskets

    The optional torque wrench is available   here to avoid overtightening the flange bolts

    Heating Element

    Fe-Cr-Al Alloy doped by Mo

    Application Notes   

    Hytort Application, or named   Hydroretorting of Shale Oil is a process developed by IGT to double the yield   of shale oil and hydrocarbon gasses. Please click underlined to view research   paper

    Attention: A two-stage pressure regulator   must be installed on the gas cylinder to limit the gas output pressure to the   below the safety limit. The pressure regulator is not included. Please click   here to learn how to install the gas regulator.

    Safety Notes

    Ni-based Superalloy: ( Waspaloy or   equivalent is a reliable processing tube which can be used under high temperature   and high pressure. It has excellent ductility and tensile property so only   creep deformation happens under overpressure destruction test and following   by a crack formed (usually at the hot zone at the center of the tube) to   release the pressure. Brittle fracture won’t happen in the overpressure   destruction test which means no tube explosion will happen under the   overpressure of inert gas or safe gas or under other accidents causing   overpressure of inert gas or safe gas.

    Attention: for the use of flammable,   toxic or corrosive gasses, you must contact MTI engineering group for the   consultation to know all the prerequisites and precautionary measures.

    Warning: Never put a sample inside the   tube directly without crucible or isolated foil to avoid it reacts with tube   alloy.

    Do not over-tightening the flange screws   as this may cause permanent damages to the flange or screws. Please refer to   the instructions about proper torque for installing CF flange bolts. We   recommend you use a torque wrench to tighten the screws with the flange.

    Warranty of High Pressure Furnace

    One year limited warranty (Consumable   parts such as o-rings and heating elements are not covered by the warranty,   please order the replacement at related products below.)

    Laptop, software